| Issue |
MATEC Web Conf.
Volume 329, 2020
International Conference on Modern Trends in Manufacturing Technologies and Equipment: Mechanical Engineering and Materials Science (ICMTMTE 2020)
|
|
|---|---|---|
| Article Number | 02015 | |
| Number of page(s) | 6 | |
| Section | Materials Science | |
| DOI | https://doi.org/10.1051/matecconf/202032902015 | |
| Published online | 26 November 2020 | |
Influence of rare earth elements on the structure and properties of powders based on zirconium dioxide during consolidation
Perm National Polytechnic University, 614990, Perm, Russia
* Corresponding author:svetlana.iron@yandex.ru
Zirconium oxide powders with different contents of REE concentrate (La, Nd, Pr) in an amount from 25 to 35 mol. % were synthesized by the method of reverse chemical deposition. The effect of the annealing temperature in the range of 600–1200 ° C on the phase transformations of the synthesized powders has been investigated by Raman spectroscopy. It was found that the formation of REE zirconates with a pyrochlore structure occurs after annealing at a temperature of 1000 ° C. At higher annealing temperatures, the presence of tetragonal ZrO2 was noted in the samples with a lower concentrate content in the phase composition. A study of the influence of the sintering temperature of 1400-1600 °C on the densification processes, phase composition and microstructure of ceramic materials based on REE zirconates has been carried out. It has been shown that the densification processes proceed most slowly in a ceramic material with 35 mol.% of rare-earth oxides, and at all sintering temperatures it has a stable phase composition, consisting mainly of rare-earth zirconates with a pyrochlore structure.
© The Authors, published by EDP Sciences, 2020
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