Influence of the quenching rate and step-wise cooling temperatures on microstructural and tensile properties of PER72 ® Ni-based superalloy

¹ Université de Toulouse; Mines Albi, INSA, UPS, ISAE; ICA (Institut Clément Ader), Campus Jarlard, 81013 Albi Cedex 09, France
² Aubert & Duval, BP. 1, 63770 Les Ancizes, France

Abstract

The PER72® grade is used as a wrought engine turbine disk, which is a critical high temperature component. During the heat treatment process, residual stresses are generated during the quench, which may lead to irreversible damages on the workpiece. The aim of this study is to better understand the mechanisms involved in the residual stress generation. Therefore, the influence of quenching conditions on the high temperature tensile properties and the multi-scale microstructure evolutions are investigated after cooling. PER72® specimens are annealed above the solvus temperature, directly on the servo-hydraulic testing machine. Three quenching rates are used: 30 ^∘C/min, 120 ^∘C/min, and 300 ^∘C/min. For each condition, the cooling is interrupted at 1000 ^∘C, 850 ^∘C, 600 ^∘C and 20 ^∘C to perform isothermal tensile test. Specimens are post-mortem analysed. On one hand the fracture surface is investigated using SEM. On the other hand the microstructure evolution was observed and quantified at different scales using SEM directly on the bulk or after the chemical extraction of precipitation. The precipitation size and volume fraction statistics, X-Ray diffraction for the crystallography and composition of the different phases are investigated. It was shown that the testing temperature does not significantly influence the γ′ distribution of particles. Conversely, the γ′ precipitation is strongly influenced by the cooling rate. Notably, the average size, the distance between particles as well as the number density of γ′ precipitates are significantly modified by the cooling rate. Changes in tensile properties are related to microstructural.