MATEC Web Conf.
Volume 142, 2018International Conference on Materials Applications and Engineering 2017 (ICMAE2017)
|Number of page(s)||6|
|Section||Chemical Materials and Chemical Syntheses|
|Published online||08 January 2018|
Determination of Nickel in End-Fitting of Spoolable Reinforced Plastic Line Pipe
State Key Laboratory for Performance and Structure Safety of Petroleum Tubular Goods and
Equipment Materials, No. 89 Jinyeer Road, Xi’an 710077, China
2 CNPC Tubular Goods Research Institute, No. 89 Jinyeer Road, Xi’an 710077, China
* Corresponding author: email@example.com
Spoolable reinforced plastic line pipe will be widely used in the exploitation of acid gas and oil wells. End-fitting is a mechanical device that forms the transition from the spoolable reinforced plastic line pipe to the connector. It was well known that nickel was an important element in the end-fitting. In this paper, a novel spectrophotometric method was described for determination of nickel in the end-fitting of spoolable reinforced plastic line pipe. The method was based on the color reaction between nickel and dimethylglyoxime, which was favored in an alkaline medium, producing a red compound in the presence of ammonium persulfate as an oxidant. Under the optimum reaction conditions the absorption value was proportional to the concentration of nickel in the range of 0.080~0.50% (R2 = 0.9999), and the relative standard deviation was less than 3.0% (n=5). The proposed method was applied successfully to determine nickel in end-fitting of spoolable reinforced plastic line pipe.
© The Authors, published by EDP Sciences, 2018
This is an Open Access article distributed under the terms of the Creative Commons Attribution License 4.0, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (http://creativecommons.org/licenses/by/4.0/).
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